Dalton Trans., 2012, Advance Article
DOI: 10.1039/C2DT30505D, Paper
DOI: 10.1039/C2DT30505D, Paper
Christopher C. Brown, Douglas W. Stephan
Thermal reaction of 1 : 1 mixtures of the RuCl2(PPh3)3 and phosphinoimine R2PN[double bond, length as m-dash]CPh2 (R = Ph, iPr, Me) at 140 [degree]C results in isolation of the dimeric species [RuCl([small mu ]-Cl)(PPh3)(C6H4(PPh2)C(Ph)NH)]2 (R = Ph 1, iPr 2, Me 3) containing phosphine-imine chelating ligands.
Thermal reaction of 1 : 1 mixtures of the RuCl2(PPh3)3 and phosphinoimine R2PN[double bond, length as m-dash]CPh2 (R = Ph, iPr, Me) at 140 [degree]C results in isolation of the dimeric species [RuCl([small mu ]-Cl)(PPh3)(C6H4(PPh2)C(Ph)NH)]2 (R = Ph 1, iPr 2, Me 3) containing phosphine-imine chelating ligands.
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